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Instruments / Technical Area	Publication Details	Published	Actions
I18-Microfocus Spectroscopy	Combining µXANES and µXRD mapping to analyse the heterogeneity in calcium carbonate granules excreted by the earthworm Loredana Brinza , Paul Schofield , Mark Hodson , Sophie Weller , Konstantin Ignatyev , Kalotina Geraki , Paul Quinn , J. Frederick W. Mosselmans Journal Of Synchrotron Radiation 21, 235 - 241 DOI: 10.1107/S160057751303083X PMID: 24365942 Diamond Proposal Number(s): [7755, 3895] Open Access Show Abstract ▼ Abstract: The use of fluorescence full spectral micro-X-ray absorption near-edge structure (µXANES) mapping is becoming more widespread in the hard energy regime. This experimental method using the Ca K-edge combined with micro-X-ray diffraction (µXRD) mapping of the same sample has been enabled on beamline I18 at Diamond Light Source. This combined approach has been used to probe both long- and short-range order in calcium carbonate granules produced by the earthworm Lumbricus terrestris. In granules produced by earthworms cultured in a control artificial soil, calcite and vaterite are observed in the granules. However, granules produced by earthworms cultivated in the same artificial soil amended with 500 p.p.m. Mg also contain an aragonite. The two techniques, µXRD and µXANES, probe different sample volumes but there is good agreement in the phase maps produced.	Jan 2014

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