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Instruments / Technical Area	Publication Details	Published	Actions
I12-JEEP: Joint Engineering, Environmental and Processing	Following the electroreduction of uranium dioxide to uranium in LiClKCl eutectic in situ using synchrotron radiation L D Brown , Rema Abdulaziz , Rhodri Jervis , Vidal Bharath , R C Attwood , Christina Reinhard , Leigh Connor , S J R Simons , D. Inman , D J L Brett , Paul Shearing Journal Of Nuclear Materials 464, 256 - 262 DOI: 10.1016/j.jnucmat.2015.04.037 Diamond Proposal Number(s): [9690] Open Access Show Abstract ▼ Abstract: The electrochemical reduction of uranium dioxide to metallic uranium has been investigated in lithium chloridepotassium chloride eutectic molten salt. Laboratory based electrochemical studies have been coupled with in situ energy dispersive X-ray diffraction, for the first time, to deduce the reduction pathway. No intermediate phases were identified using the X-ray diffraction before, during or after electroreduction to form α-uranium. This suggests that the electrochemical reduction occurs via a single, 4-electron-step, process. The rate of formation of α-uranium is seen to decrease during electrolysis and could be a result of a build-up of oxygen anions in the molten salt. Slow transport of O2− ions away from the UO2 working electrode could impede the electrochemical reduction.	Sep 2015

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