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Instruments / Technical Area	Publication Details	Published	Actions
I19-Small Molecule Single Crystal Diffraction	Contrasting crystal packing arrangements in triiodide salts of radical cations of chiral bis(pyrrolo[3,4-d])tetrathiafulvalenes Lee Martin , Songjie Yang , Andrew C. Brooks , Peter Horton , Louise Male , Ourida Moulfi , Lydie Harmand , Peter Day , William Clegg , Ross W. Harrington , John D. Wallis Crystengcomm 17 (38), 7354-7362 DOI: 10.1039/C5CE01430A Diamond Proposal Number(s): [987] Open Access Show Abstract ▼ Abstract: Crystal structures of six 1 : 1 triiodide salts of a series of enantiopure bisĲpyrroloĳ3,4-d])TTF derivatives, the first structures of radical cation salts reported for this bisĲpyrrolo) donor system, show three different arrangements of triiodide ions, organised either in head-to-tail pairs, in infinite lines, or in a castellated arrangement. The complex crystal structures, obtained by electrocrystallisation, are influenced by the presence of solvent, for example changing an ABCABC packing arrangement to ABAB with inclusion of THF, as well as by the size of the chiral side chain.	Aug 2015

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