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Instruments / Technical Area	Publication Details	Published	Actions
B18-Core EXAFS	Design of Highly Selective Platinum Nanoparticle Catalysts for the Aerobic Oxidation of KA-Oil using Continuous-Flow Chemistry Arran M. Gill , Christopher Hinde , Rowan K. Leary , Matthew Potter , Andrea Jouve , Peter Wells , Paul A. Midgley , John M. Thomas , Robert Raja Chemsuschem DOI: 10.1002/cssc.201501264 Diamond Proposal Number(s): [8071] Show Abstract ▼ Abstract: Highly active and selective aerobic oxidation of KA-oil to cyclohexanone (precursor for adipic acid and ɛ-caprolactam) has been achieved in high yields using continuous-flow chemistry by utilizing uncapped noble-metal (Au, Pt & Pd) nanoparticle catalysts. These are prepared using a one-step in situ methodology, within three-dimensional porous molecular architectures, to afford robust heterogeneous catalysts. Detailed spectroscopic characterization of the nature of the active sites at the molecular level, coupled with aberration-corrected scanning transmission electron microscopy, reveals that the synthetic methodology and associated activation procedures play a vital role in regulating the morphology, shape and size of the metal nanoparticles. These active centers have a profound influence on the activation of molecular oxygen for selective catalytic oxidations.	Feb 2016

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