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Instruments / Technical Area	Publication Details	Published	Actions
B18-Core EXAFS I11-High Resolution Powder Diffraction I15-Extreme Conditions	Amorphous silicate nanoparticles with controlled Fe-Mg pyroxene compositions Stephen Thompson , Karine Demyk , Sarah Day , Aneurin Evans , Hugues Leroux , Christophe Depecker , Julia Parker , Leigh Connor , Heribert Wilhelm , Giannantonio Cibin Journal Of Non-Crystalline Solids 447, 255 - 261 DOI: 10.1016/j.jnoncrysol.2016.06.017 Diamond Proposal Number(s): [8614, 8692] Show Abstract ▼ Abstract: The production of amorphous pyroxene nanoparticles (~20 nm) with controlled Fe-Mg content is described. Homogenous particle compositions closely matching required target stoichiometries are obtained by drying a precursor gel under high vacuum conditions. The silicate nature of the particles is characterised using TEM, synchrotron radiation and FTIR. No oxide phase separation occurs, even at high Fe concentration. Structural domains exist within the nanoparticles that are typically ten times smaller than the physical particle size consistent with either a core-shell, or, random network with multiple embedded domains, particle structure. Thermal annealing below the crystallisation temperature allows the ordered domain size to be further reduced by a factor of ~2.	Sep 2016

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