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Instruments / Technical Area	Publication Details	Published	Actions
I19-Small Molecule Single Crystal Diffraction	An electric field cell for performing in situ single-crystal synchrotron X-ray diffraction Lucy K. Saunders , Hamish H.-M. Yeung , Mark Warren , Peter Smith , Stuart Gurney , Stephen F. Dodsworth , Inigo Vitorica-Yrezabal , Adrian Wilcox , Paul V. Hathaway , Geoff Preece , Paul Roberts , Sarah A. Barnett , David R. Allan Journal Of Applied Crystallography 54 DOI: 10.1107/S1600576721007469 Diamond Proposal Number(s): [19670, 22964] Open Access Show Abstract ▼ Abstract: With the recent increase in research into ferroelectric, anti-ferroelectric and piezoelectric materials, studying the solid-state properties in situ under applied electric fields is vital in understanding the underlying processes. Where this behaviour is the result of atomic displacements, crystallographic insight has an important role. This work presents a sample environment designed to apply an electric field to single-crystal samples in situ on the small-molecule single-crystal diffraction beamline I19, Diamond Light Source (UK). The configuration and operation of the cell is described as well as its application to studies of a proton-transfer colour-change material.	Oct 2021
I15-Extreme Conditions	Laser-heating system for high-pressure X-ray diffraction at the Extreme Conditions beamline I15 at Diamond Light Source Simone Anzellini , Annette K. Kleppe , Dominik Daisenberger , Michael T. Wharmby , Ruggero Giampaoli , Silvia Boccato , Marzena A. Baron , Francesca Miozzi , Dean S. Keeble , Allan Ross , Stuart Gurney , Jon Thompson , Giles Knap , Mark Booth , Lee Hudson , Dave Hawkins , Michael J. Walter , Heribert Wilhelm Journal Of Synchrotron Radiation 25 DOI: 10.1107/S1600577518013383 Open Access Show Abstract ▼ Abstract: In this article, the specification and application of the new double-sided YAG laser-heating system built on beamline I15 at Diamond Light Source are presented. This system, combined with diamond anvil cell and X-ray diffraction techniques, allows in situ and ex situ characterization of material properties at extremes of pressure and temperature. In order to demonstrate the reliability and stability of this experimental setup over a wide range of pressure and temperature, a case study was performed and the phase diagram of lead was investigated up to 80 GPa and 3300 K. The obtained results agree with previously published experimental and theoretical data, underlining the quality and reliability of the installed setup.	Nov 2018

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