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Instruments / Technical Area	Publication Details	Published	Actions
I19-Small Molecule Single Crystal Diffraction	Nanometer control in plasmonic systems through discrete layer-by-layer macrocycle–cation deposition Steven J. Barrow , Aniello Palma , Bart De Nijs , Rohit Chikkaraddy , Richard W. Bowman , Jeremy J. Baumberg , Oren A. Scherman Nanoscale 12, 8706 - 8710 DOI: 10.1039/D0NR00902D Show Abstract ▼ Abstract: In this work, we demonstrate that coordination interactions between Fe3+ and cucurbit[7]uril (CB[7]) can be utilised to build up defined nanoscale spacing layers in metallic nanosystems. We begin by characterising the layer-by-layer deposition of CB[7] and FeCl3·6H2O coordination layers through the use of a Quartz-Crystal Microbalance (QCM) and contact angle measurements. We then apply this layered structure to accurately control the spacing, and thus optical properties, of gold nanoparticles in a Nanoparticle-on-Mirror (NPoM) structure, which is demonstrated via normalising plasmon resonance spectroscopy.	Apr 2020
I19-Small Molecule Single Crystal Diffraction	Photocontrol over cucurbit[8]uril complexes: stoichiometry and supramolecular polymers Jesús Del Barrio , Peter Horton , Didier Lairez , Gareth O. Lloyd , Chris Toprakcioglu , Oren A. Scherman Journal Of The American Chemical Society 135 (32), 11760 - 11763 DOI: 10.1021/ja406556h Diamond Proposal Number(s): [8521] Show Abstract ▼ Abstract: Herein we report the photocontrol of cucurbit[8]uril (CB[8])-mediated supramolecular polymerization of azobenzene-containing monomers. The CB[8] polymers were characterized both in solution and in the solid state. These host–guest complexes can be reversibly switched between highly thermostable photostationary states. Moreover, a remarkable stabilization of Z-azobenzene was achieved by CB[8] complexation, allowing for structural characterization in the solid state.	Jul 2013

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