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I09-Surface and Interface Structural Analysis	Spontaneous lithiation of binary oxides during epitaxial growth on LiCoO2 Le Wang , Zhenzhong Yang , Widitha S. Samarakoon , Yadong Zhou , Mark E. Bowden , Hua Zhou , Jinhui Tao , Zihua Zhu , Nabajit Lahiri , Timothy C. Droubay , Zachary W. Lebens-Higgins , Xinmao Yin , Chi Sin Tang , Zhenxing Feng , Louis F. J. Piper , Andrew T. S. Wee , Scott A. Chambers , Yingge Du Nano Letters 9 DOI: 10.1021/acs.nanolett.2c01701 Diamond Proposal Number(s): [19162] Show Abstract ▼ Abstract: Epitaxial growth is a powerful tool for synthesizing heterostructures and integrating multiple functionalities. However, interfacial mixing can readily occur and significantly modify the properties of layered structures, particularly for those containing energy storage materials with smaller cations. Here, we show a two-step sequence involving the growth of an epitaxial LiCoO2 cathode layer followed by the deposition of a binary transition metal oxide. Orientation-controlled epitaxial synthesis of the model solid-state-electrolyte Li2WO4 and anode material Li4Ti5O12 occurs as WO3 and TiO2 nucleate and react with Li ions from the underlying cathode. We demonstrate that this lithiation-assisted epitaxy approach can be used for energy materials discovery and exploring different combinations of epitaxial interfaces that can serve as well-defined model systems for mechanistic studies of energy storage and conversion processes.	Jun 2022

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