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I22-Small angle scattering & Diffraction	Synthesis of core-shell polymer particles in supercritical carbon dioxide via iterative monomer addition Kristoffer Konrad Kortsen , Morgan Reynolds-Green , Bradley Hopkins , Allison Mclellan , Matthew J. Derry , Paul D. Topham , Jeremy J. Titman , Daniel J. Keddie , Vincenzo Taresco , Steven M. Howdle Chemical Communications DOI: 10.1039/D3CC04969H Diamond Proposal Number(s): [33098] Open Access Show Abstract ▼ Abstract: A new, robust methodology for the synthesis of polystyrene-poly(methyl methacrylate) (PS-PMMA) core-shell particles using seeded dispersion polymerisation in supercritical carbon dioxide is reported, where the core-shell ratio can be controlled predictably via manipulation of reagent stoichiometry. The key development is the application of an iterative addition of the MMA shell monomer to the pre-prepared PS core. Analysis of the materials with differing core-shell ratios indicate that all are isolated as single particle populations with distinct and controllable core-shell morphologies.	Nov 2023

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