Mechanical Engineering
Survey
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Sep 2009
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Mechanical Engineering
Vacuum
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Open Access
Abstract: The project required a sample environment to deliver experiments
in vacuum or helium, with high humidity, including
capacity to use aggressive solvents. The compact, transportable
system incorporates a high precision in-vacuum
manipulator/ positioning stage (with repeatability better than
1 μm/ 1 mdeg) allowing for multiple sample configurations.
Current sample mounts include in-situ film formation (Doctor
Blade), thermal annealing/drying heater stage, sample
cooling and multiple sample stages; the system has been
designed to accommodate many sample substrate formats.
The existing end station camera system has been upgraded
to include two, in-vacuum, WAXS and SAXS area detectors,
which are custom builds based on the Pilatus 6M. The
SAX detector module includes three in vacuum, independent
,configurable SAXS beam stop manipulators to block
GISAXS transmitted, reflected and specular flare as well as
isotropic and anisotropic SAX, a photon sensitive detector
shutter plate is included. The 4mm diameter tungsten beam
stops each include a miniature photodiode to measure beam
intensity and can be positioned to within 10 μm precision in
X and Y over 300mm x 250mm motion range.
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Jun 2017
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NONE-No attached Diamond beamline
Metrology
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Jun 2006
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Metrology
Optics
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Abstract: In January 2007, Diamond Light Source (DLS) Ltd, the new 3rd generation national synchrotron source for the UK, welcomed its first scientific users. The successful exploitation of the intense synchrotron light produced by DLS will depend to a significant extent on the quality and performance of the optics employed in the experimental stations (beamlines). An in-house facility is required for acceptance and optimization of synchrotron optics, and for fundamental research to develop new technologies. A cleanroom laboratory has been constructed at DLS to house a suite of metrology instruments capable of characterizing state-of-the-art, synchrotron optics. A micro-interferometer and an atomic force microscope, with capability to integrate the two devices, are used to assess the atomic scale roughness of x-ray optics. A Fizeau interferometer and a slope measuring profiling system are used to measure the larger scale topography of sample surfaces. These non-contact, complementary techniques allow a broad spectrum of lateral features, from 1nm to 1m, to be probed to high accuracies. We present metrology data obtained using the instruments listed above.
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Sep 2007
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Metrology
Optics
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Abstract: The Diamond Optics & Metrology Group and the collaborators at the STFC Central Microstructure Facility have initiated a program for the design and fabrication of in-line micro- and nano-focusing optics for synchrotron radiation beamlines. The first type of optics fabricated is a kinoform lens in silicon on the same model proposed by K. Evans- Lutterodt et al [Opt. Expr. 11 (2003) 919.]. The fabrication utilised ultra high resolution electron beam lithographic patterning of an electron sensitive SU8 polymer and deep reactive ion etching of silicon. The first test of the focusing properties was performed at the ESRF BM5 optics beamline. In this paper we present details on the design and fabrication, and discuss the test results.
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Aug 2007
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Metrology
Optics
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Open Access
Abstract: We present a comprehensive investigation of the systematic and random errors of the nano-metrology instruments used to characterize synchrotron X-ray optics at Diamond Light Source. With experimental skill and careful analysis, we show that these instruments used in combination are capable of measuring state-of-the-art X-ray mirrors. Examples are provided of how Diamondmetrology data have helped to achieve slope errors of <100 nrad for optical systems installed on synchrotron beamlines, including: iterative correction of substrates using ion beam figuring and optimal clamping of monochromator grating blanks in their holders. Simulations demonstrate how random noise from the Diamond-NOM’s autocollimator adds into the overall measured value of the mirror’s slope error, and thus predict how many averaged scans are required to accurately characterize different grades of mirror.
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May 2016
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Metrology
Optics
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Open Access
Abstract: The shapes of single lens surfaces capable of focusing divergent and collimated beams without aberration have already been calculated. However, nanofocusing compound refractive lenses (CRLs) require many consecutive lens surfaces. Here a theoretical example of an X-ray nanofocusing CRL with 48 consecutive surfaces is studied. The surfaces on the downstream end of this CRL accept X-rays that are already converging toward a focus, and refract them toward a new focal point that is closer to the surface. This case, so far missing from the literature, is treated here. The ideal surface for aberration-free focusing of a convergent incident beam is found by analytical computation and by ray tracing to be one sheet of a Cartesian oval. An `X-ray approximation' of the Cartesian oval is worked out for the case of small change in index of refraction across the lens surface. The paraxial approximation of this surface is described. These results will assist the development of large-aperture CRLs for nanofocusing.
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Nov 2017
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Metrology
Optics
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Abstract: This thesis presents research and development work on synchrotron X-ray atwavelength
metrology methods. Two approaches for measuring the phase of an Xray
wavefront were studied: the grating-based and the speckle-based methods. The
X-ray grating interferometer is the most widespread technique representative of the
first category. Its performance and potential in various situations encountered in atwavelength
metrology were investigated. Speckle methods are X-ray phase sensing
techniques newly developed during this thesis project. They make use of membranes
with small features, whose statistical distribution is the only known specification, to
modulate the beam wavefront. The different methods were deployed experimentally
at the beamlines BM05 of the ESRF and B16 of the Diamond Light Source. Their
implementation permitted the characterization of various kinds of optical elements
used to manipulate synchrotron X-ray beams as well as the feasibility study of micro
phase contrast imaging using the two methods described above.
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May 2013
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Metrology
Optics
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Carolyn
Atkins
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Charlotte
Feldman
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David
Brooks
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Stephen
Watson
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William
Cochrane
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Mélanie
Roulet
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Emmanuel
Hugot
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Mat
Beardsley
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Christopher
Spindloe
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Simon
Alcock
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Ioana-theodora
Nistea
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Christian
Morawe
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Francois
Perrin
,
Michael
Harris
Abstract: Additive manufacturing (AM), more commonly known as 3D printing, is a commercially established technology for rapid prototyping and fabrication of bespoke intricate parts. To date, research quality mirror prototypes are being trialled using additive manufacturing, where a high quality reflective surface is created in a post-processing step. One advantage of additive manufacturing for mirror fabrication is the ease to lightweight the structure: the design is no longer confined by traditional machining (mill, drill and lathe) and optimised/innovative structures can be used. The end applications of lightweight AM mirrors are broad; the motivation behind this research is low mass mirrors for space-based astronomical or Earth Observation imaging. An example of a potential application could be within nano-satellites, where volume and mass limits are critical. The research presented in this paper highlights the early stage experimental development in AM mirrors and the future innovative designs which could be applied using AM. The surface roughness on a diamond-turned AM aluminium (AlSi10Mg) mirror is presented which demonstrates the ability to achieve an average roughness of ~3.6nm root mean square (RMS) measured over a 3 x 3 grid. A Fourier transform of the roughness data is shown which deconvolves the roughness into contributions from the diamond-turning tooling and the AM build layers. In addition, two nickel phosphorus (NiP) coated AlSi10Mg AM mirrors are compared in terms of surface form error; one mirror has a generic sandwich lightweight design at 44% the mass of a solid equivalent, prior to coating and the second mirror was lightweighted further using the finite element analysis tool topology optimisation. The surface form error indicates an improvement in peak-to-valley (PV) from 323nm to 204nm and in RMS from 83nm to 31nm for the generic and optimised lightweighting respectively while demonstrating a weight reduction between the samples of 18%. The paper concludes with a discussion of the breadth of AM design that could be applied to mirror lightweighting in the future, in particular, topology optimisation, tessellating polyhedrons and Voronoi cells are presented.
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Jul 2018
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Metrology
Optics
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Open Access
Abstract: Piezoelectric bimorph deformable mirrors (`bimorphs') are routinely used on many synchrotron and free-electron laser beamlines to provide active variation in the size and shape of the X-ray beam. However, the time-domain potential of such optics has never been fully exploited. For the first time, the fast dynamic bending response of bimorphs is investigated here using Fizeau interferometry. Automated scripts for acquisition and analysis were developed to collect Fizeau data at a rate of 0.1 Hz to record dynamic changes in the optical surface as voltages were applied to the electrodes of the piezoelectric actuators. It is demonstrated that residual drift in the tangential radius of curvature of a bimorph can be significantly reduced using enhanced opto-mechanical holders and a fast programmable high-voltage power supply. Further improvements are achieved by applying small opposing voltages to compensate for piezoelectric creep. The present study shows that bimorphs can truly be used as high-speed adaptive optics for the X-ray domain, even without closed-loop feedback correction. This opens the possibility for relatively simple real-time tuning of the profile of X-ray bimorphs. Part II of this study [Alcock, Nistea, Signorato, Owen, Axford, Sutter, Foster & Sawhney (2019), J. Synchrotron Rad. 26, this issue] builds upon these results and demonstrates how bimorphs can rapidly provide customisable sizes and shapes of synchrotron X-ray beams, specifically tailored to suit the experimental samples being investigated.
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Dec 2018
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